李玉荃,王亚江,刘志友,叶俊杰,缪子敬.布南色林的单晶培养和结构确证[J].现代药物与临床,2011,26(3):216-218
布南色林的单晶培养和结构确证
Single crystal culture and structure confirmation of Blonanserin
  
DOI:10.7501/j.issn.1674-5515.[year].[issue].[sequence]
中文关键词:  布南色林  单晶  X射线单晶衍射  空间结构
英文关键词:Blonanserin  single crystal  X-ray single crystal diffraction  space structure
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作者单位E-mail
李玉荃 天津市医药集团技术发展有限公司天津 300193 liyq@tjipr.com 
王亚江,刘志友,叶俊杰,缪子敬   
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中文摘要:
      目的 培养布南色林的单晶,以验证所合成的化合物为布南色林。方法 通过温度、质量浓度、溶剂的考察,选择合适的条件,培养出大小适合X射线单晶衍射检测的布南色林单晶。结果 通过X射线单晶衍射测定,结果显示所得数据与文献报道一致,证明布南色林的化学结构正确。结论 采用本法可很好地获得大小适合X射线单晶衍射检测的布南色林单晶,并确证了其空间结构,提示合成的布南色林结构正确。
英文摘要:
      Objective To cultivate the single crystal of Blonanserin, and to establish the structure of Blonanserin. Method To selected the best condition by inspecting the different temperature, concentration, and solution. At this condition the single crystal size of Blonanserin fit for X-ray analysis. Results The structure of Blonanserin was accurate and the data was the same with the literature report. It proved that the structure of Blonanserin was right. Conclusion The single crystal size of Blonanserin obtained is fit for X-ray analysis and the space structure is proved right. And it suggests the structure that synthesized by our corporation be exact.
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